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Tributylamine ion paired reversed phase LC/MS As previously reported 9,10,27,57 , mobile phase A was LC/MS H 2 O (W6-4, Fisher) with 3% LC/MS grade MeOH (A456-4, Fisher), mobile phase B was LC/MS grade methanol (A456-4, Fisher), and both mobile phases contained 10 mM tributylamine (90780-100 ML, Sigma), 15 mM acetic acid, and 0.01% medronic acid (v/v, 5191-4506, Agilent)

* Correspondence: Abdalsalam Kmail, [email protected] Disclaimer All claims expressed in this article are solely those of the authors and do not necessarily represent those of their affiliated organizations, or those of the publisher, the editors and the reviewers
Hyperthyroidism can also interrupt sleep by increasing heart rate and resulting in fatigue

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